High-Performance Liquid Chromatograph Primaide
Hitachi Primaide™ PM1110 isocratic pump, programmable
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The Primaide1110 Pump has been developed for reliable analysis and shares characteristics with Hitachi's existing HPLC pump models. Its consistently high level of performance provides users with strong support in everyday analysis.
Improvement of flow rate stability
For pulse compensation, a proprietary real-time feedback method has been developed for Hitachi’s pumps. Not only has the pulse has been significantly reduced, but the Primaide1110 Pump estimates pressure fluctuations and employs the optimal timing to set the plunger speed interval.
Improvement of retention time reproducibility
For gradient analysis, injection by the Primaide1210 Autosampler is synchronized with the movements of the pump. This ensures a highly-reproducible retention time, and guarantees precise analysis.
Built-in optional units inside pump
Both the degasser and gradient unit can be mounted inside the pump. A built-in degasser minimizes the tubing volume, and yields a more compact system by eliminating the need for additional modules. The gradient unit is capable of mixing 4 solvents via its solenoid valves. The placement of the mixer in a high-pressure compartment enables high-precision, stable mixing, even with a single pump.
Gradient Performance Evaluation/RT and Area Reproducibility
Peak No. | Component | Retention Time | |
Average / min. | R.S.D. / % | ||
1 | Acetanilide | 2.032 | 0.076 |
2 | Acetophenone | 2.793 | 0.080 |
3 | Propiophenone | 3.581 | 0.096 |
4 | Butyrophenone | 4.495 | 0.102 |
5 | Benzophenone | 4.809 | 0.098 |
6 | Valerophenone | 5.639 | 0.083 |
7 | Hexanophenone | 6.975 | 0.082 |
8 | Heptanophenone | 8.413 | 0.068 |
9 | Octanophenone | 9.882 | 0.078 |
Condition | |
Column | HITACHI LaChrom C18 (5 µm) 4.6 mm I.D.×150 mm L. |
Mobile phase | A : CH3OH B : H2O |
Gradient program | 0 - 11 min A 65 → 100% |
Column Temperature | 40°C |
Flow rate | 1.0 mL/min |
Detection | UV 265 nm |
Injection vol. | 10 µL (100 g/mL each.) |
SPECIFICATIONS
Liquid feed system | Dual plunger reciprocating pump (series connection, pulsation suppression) |
Flow rate range | 0.001 to 9.999 mL/min. |
Maximum discharge pressure | 39.2 MPa (0.001 to 5.000 mL/min.) 19.6 MPa (5.001 to 9.999 mL/min.) |
Flow rate accuracy | ±2 μL/min. (0.01 to 0.1 mL/min.) ±2 % (0.101 to 8.0 mL/min.) ±4 % (8.001 to 9.999 mL/min.) |
Flow rate stability | SD 0.02min. or RSD 0.075 %, whichever is larger (retention time at 1.0 mL/min.) |
Dimensions/weight | 340(W) × 464(D) × 159(H) mm, approx. 13.0 kg |
ADDITIONAL OPTIONS:
- Degasser®
- Low-pressure gradient unit
- Pump seal washing kit
- UI-Pad
- Model: Iso-PM1110
- Manufactured by: Merck Hitachi